Three folders of raw data in open readable format. Datasets for PXRD, XPS, and EXAFS. 

PXRD for Ni/CeO2-SA and Ni/CeO2-NC (Fresh, post reaction, and reduced) in .xy format. Collected at Diamond Light Source with access to beamline I11 for PXRD measurements (Proposal CY31578). 

XPS reports and data for Ni/CeO2-SA and Ni/CeO2-NC (Fresh, post reaction, and reduced) in readable files. Collected at EPSRC National Facility for XPS (“HarwellXPS”, EP/Y023587/1, EP/Y023609/1, EP/Y023536/1, EP/Y023552/1 and EP/Y023544/1). 

EXAFS data (Raw unprocessed data and processed R, Q, K plots for NiO, Ni, Ni/CeO2-SA and Ni/CeO2-NC (Fresh and post reaction) in .dat extension. Collected at Diamond Light Source on beamline B18 through the UK Catalysis Hub BAG (Proposal SP29271). 