============
MestRe-C
============
Title:4mm HXY probe. 1H-31P-15N, 31P-13C/15N insert. low range mode, using X preamp for Y channel observing

15N CP

sample: VP CN 20

ref to NH2 of glycine at 33.8 ppm, sr = 809.22 Hz

MAS = 5kHz

1H rf = 3us, 83kHz, 7.5dB

15N rf = 6.2us, 40kHz, 7.26dB

1H contact  4.2us, 60kHz, 10.5dB matched to 15N at 40 kHz, 7.26 dB

contact time = 6ms

1H decoupling = 83khz, 7.50dB

aq = 40ms


























































































































































Spectrometer Frequency =	40.5134
Sweep Width =	50125.3133
Time domain=	2048
Units=	ppm
Real Data Points Output
=====================================================
651.708	33912.2930
650.500	131968.1406
649.291	41666.6016
648.083	58511.4766
646.875	76397.6953
645.667	60492.4180
644.458	44446.6406
643.250	25371.0586
642.042	73166.7578
640.834	44173.7227
639.625	64056.3477
638.417	32051.3398
637.209	84564.5469
636.001	15426.2500
634.792	-56857.4648
633.584	116076.9453
632.376	57410.1016
631.168	64122.6875
629.959	12732.6602
628.751	45762.6289
627.543	-15074.5811
626.335	62160.5156
625.126	102935.1406
623.918	-16186.3223
622.710	-96681.4453
621.502	28734.5371
620.293	-25730.5449
619.085	79685.8828
617.877	15317.4736
616.669	11974.3896
615.460	-124732.1875
614.252	-105728.7422
613.044	5458.1484
611.836	-71989.3047
610.627	57278.7930
609.419	6997.3721
608.211	-58081.8164
607.002	-110146.8828
605.794	46515.7539
604.586	-61935.8125
603.378	55251.7734
602.169	-59112.2695
600.961	24317.9395
599.753	38058.3242
598.545	-1142.8585
597.336	41018.7891
596.128	5298.1499
594.920	-5209.5054
593.712	21226.9492
592.503	112311.0000
591.295	24946.6289
590.087	-24165.4883
588.879	-49347.6289
587.670	-45385.5977
586.462	-5605.7065
585.254	-43242.2031
584.046	39292.4492
582.837	-76380.8359
581.629	94577.7031
580.421	124124.4609
579.213	-29194.6797
578.004	40472.6719
576.796	-59589.5938
575.588	22611.9727
574.380	67170.5156
573.171	-53662.3867
571.963	-39441.9492
570.755	28609.6250
569.547	-26451.8184
568.338	-36879.5508
567.130	-69879.9141
565.922	1460.5740
564.714	46833.8750
563.505	-15194.9268
562.297	115286.2109
561.089	-111164.8984
559.881	7657.7769
558.672	39384.5078
557.464	-4816.4688
556.256	-55265.4688
555.048	1332.1042
553.839	-10400.4805
552.631	-39539.6602
551.423	11906.3535
550.215	32494.4082
549.006	-70238.2656
547.798	-91119.0078
546.590	-78151.2969
545.382	-128630.6172
544.173	-59976.8711
542.965	-85967.5156
541.757	-43370.2617
540.549	-13883.4023
539.340	-49240.4922
538.132	-111336.5703
536.924	-112897.7344
535.715	3204.6824
534.507	-30857.2363
533.299	25488.7148
532.091	-6734.1909
530.882	-80784.8672
529.674	-64876.0391
528.466	-28909.8594
527.258	-59388.9336
526.049	27587.8301
524.841	-49695.7500
523.633	-57316.8750
522.425	-57547.1133
521.216	29873.9219
520.008	3617.6223
518.800	-54714.1016
517.592	50303.4336
516.383	-87409.0703
515.175	-12732.0166
513.967	-176480.1250
512.759	-88581.5781
511.550	-70093.4688
510.342	-104978.7344
509.134	-203792.7656
507.926	-7763.7920
506.717	16512.3242
505.509	-117696.7891
504.301	-6725.2788
503.093	-88329.7656
501.884	-20235.9043
500.676	-53349.1797
499.468	-115280.0469
498.260	-9757.5186
497.051	18571.7949
495.843	-65961.3750
494.635	-21941.0156
493.427	-114048.9766
492.218	14749.7295
491.010	-106181.8516
489.802	-91849.5625
488.594	-35471.6680
487.385	-16176.1230
486.177	-52430.7656
484.969	-58342.1484
483.761	-78272.1406
482.552	-18664.7363
481.344	-117260.2188
480.136	78098.0625
478.928	-21516.2227
477.719	-69573.4453
476.511	-95569.7188
475.303	-12494.0352
474.095	37750.2305
472.886	18888.5273
471.678	-140775.3906
470.470	-120287.2656
469.261	-89022.6953
468.053	-59903.4219
466.845	-157885.5156
465.637	-208308.8281
464.428	-59091.6133
463.220	-125419.4531
462.012	-81763.7500
460.804	-76101.5313
459.595	-99100.9922
458.387	-59734.3398
457.179	-94997.0547
455.971	-54501.5625
454.762	-23576.6563
453.554	-79449.0000
452.346	-98251.5469
451.138	-86257.6797
449.929	-38348.7227
448.721	30093.3379
447.513	81210.3047
446.305	-51768.3398
445.096	-56242.0039
443.888	-109373.7578
442.680	-127026.2109
441.472	-49794.8789
440.263	-81360.0000
439.055	-20726.2637
437.847	25049.9219
436.639	-34631.3828
435.430	-45215.5820
434.222	-65973.3906
433.014	-33423.4492
431.806	-91388.5000
430.597	-112174.2344
429.389	-76322.4609
428.181	-42714.4063
426.973	-66162.2969
425.764	-156200.5625
424.556	-111431.3281
423.348	-89335.1016
422.140	-130883.0938
420.931	-74567.1953
419.723	-34714.8555
418.515	-148787.3125
417.307	46414.9023
416.098	-158047.7500
414.890	-87218.3750
413.682	-123327.1719
412.474	-38944.9883
411.265	14555.5029
410.057	-38573.5156
408.849	-109854.6328
407.641	2321.6223
406.432	-142670.3750
405.224	-127226.4766
404.016	-137846.5781
402.808	-160642.7188
401.599	-129964.3438
400.391	-7135.0991
399.183	-147071.4688
397.974	43738.7031
396.766	-102056.0391
395.558	-6238.3477
394.350	-192029.1406
393.141	-108346.2656
391.933	-120532.9141
390.725	-149079.7969
389.517	-100802.6250
388.308	-84367.6094
387.100	-117857.0078
385.892	-53841.5742
384.684	-106409.6797
383.475	-33369.0742
382.267	-162306.7188
381.059	1271.2744
379.851	-94943.2969
378.642	-71917.5000
377.434	-93752.0156
376.226	-121999.0625
375.018	-212222.2031
373.809	-46735.6484
372.601	-93052.9219
371.393	-124879.1797
370.185	-67370.5078
368.976	-71828.2578
367.768	-85338.7969
366.560	-131134.3438
365.352	-106166.9141
364.143	-37472.9102
362.935	-124300.1406
361.727	-128373.9609
360.519	-56896.8359
359.310	-30626.0098
358.102	-74481.3516
356.894	-29758.9961
355.686	-167035.2188
354.477	-60673.8750
353.269	-164784.6250
352.061	-52154.8555
350.853	-135157.7344
349.644	43873.0938
348.436	-94398.2813
347.228	-98940.3281
346.020	-145434.5781
344.811	-157365.1719
343.603	-70431.9297
342.395	-38063.1133
341.187	-148836.0156
339.978	-175634.9688
338.770	-63010.4844
337.562	-29132.6211
336.354	-112024.7813
335.145	-99597.9141
333.937	-100304.0234
332.729	-52500.2070
331.521	42033.6602
330.312	1714.6195
329.104	-51294.1250
327.896	29641.1699
326.687	76373.0469
325.479	131627.2969
324.271	174500.3906
323.063	201899.5156
321.854	172548.1875
320.646	60924.3047
319.438	208177.5156
318.230	210228.5313
317.021	229698.3281
315.813	201665.3906
314.605	160600.1563
313.397	218010.1563
312.188	333513.3438
310.980	207294.4531
309.772	146428.8750
308.564	176777.4219
307.355	210185.5000
306.147	61936.9961
304.939	61665.7539
303.731	-17968.4648
302.522	98566.7813
301.314	21300.9141
300.106	22016.8047
298.898	-26601.0078
297.689	-80523.8047
296.481	33543.7227
295.273	-83264.7109
294.065	-29763.1250
292.856	-54802.8086
291.648	-75596.2734
290.440	-70009.6797
289.232	-136261.9688
288.023	-68104.5859
286.815	-105034.5000
285.607	-78878.8516
284.399	-54087.8594
283.190	-134166.1719
281.982	-62837.5000
280.774	-37245.7148
279.566	-71839.1641
278.357	-59058.6563
277.149	-33613.8398
275.941	-64593.1602
274.733	-199581.0313
273.524	-102772.5859
272.316	-109441.0000
271.108	-127048.4063
269.900	-143202.5625
268.691	-46128.3555
267.483	60322.0820
266.275	-71734.2266
265.067	-128350.7656
263.858	-82002.0391
262.650	-37557.4180
261.442	-3268.8369
260.234	-41984.7500
259.025	7747.8779
257.817	-50068.9766
256.609	-78703.4844
255.400	-78627.5859
254.192	-128890.5547
252.984	-39636.0117
251.776	-130868.9453
250.567	15445.9463
249.359	-61422.3320
248.151	-42393.7109
246.943	-41042.3594
245.734	-1933.3051
244.526	-25577.3262
243.318	-28899.7109
242.110	-54202.1250
240.901	-79790.9766
239.693	-82261.4531
238.485	-123557.8672
237.277	-31604.7148
236.068	-84747.6484
234.860	-142300.1563
233.652	-27666.4629
232.444	-50341.7891
231.235	40546.2695
230.027	30357.9121
228.819	43071.8828
227.611	114509.6797
226.402	69833.0859
225.194	56749.3047
223.986	165247.6094
222.778	97851.1641
221.569	175091.7344
220.361	179472.8125
219.153	252844.2188
217.945	202271.6250
216.736	180357.3750
215.528	174709.4219
214.320	271818.1250
213.112	332100.7813
211.903	310433.7813
210.695	428505.6250
209.487	493483.8750
208.279	648968.3125
207.070	761086.5625
205.862	756998.0625
204.654	1009647.9375
203.446	1130195.5000
202.237	1128169.5000
201.029	1314178.0000
199.821	1343983.5000
198.613	1393584.6250
197.404	1414798.8750
196.196	1481536.8750
194.988	1622603.8750
193.780	1777876.6250
192.571	1837773.2500
191.363	1824412.0000
190.155	1811775.3750
188.946	1863530.7500
187.738	1721228.3750
186.530	1589555.6250
185.322	1371792.5000
184.113	1216207.7500
182.905	1112277.0000
181.697	792204.1875
180.489	726514.5625
179.280	468358.1250
178.072	446092.3438
176.864	399808.0000
175.656	243584.1719
174.447	248239.3281
173.239	144632.3594
172.031	80717.9453
170.823	113251.8984
169.614	25200.3945
168.406	90687.1875
167.198	77487.1953
165.990	15571.9121
164.781	190528.6719
163.573	-22457.1758
162.365	143791.1875
161.157	129796.7031
159.948	182272.0469
158.740	82619.3203
157.532	353849.7813
156.324	390419.6563
155.115	345234.6250
153.907	226008.0156
152.699	322543.6250
151.491	114917.1328
150.282	196413.7969
149.074	167038.6406
147.866	349794.8125
146.658	216967.5156
145.449	466492.2188
144.241	591030.0625
143.033	575580.6250
141.825	848450.6875
140.616	1170516.8750
139.408	1680648.1250
138.200	2002324.7500
136.992	2526649.0000
135.783	2403027.7500
134.575	2049949.0000
133.367	1493072.5000
132.159	1099444.0000
130.950	696633.5000
129.742	769990.3125
128.534	697937.2500
127.326	699045.5625
126.117	730182.4375
124.909	664038.6875
123.701	628724.8125
122.493	583821.9375
121.284	633898.7500
120.076	640660.2500
118.868	775984.7500
117.659	946868.0625
116.451	1034191.3750
115.243	1081299.1250
114.035	953451.6250
112.826	904613.1250
111.618	935948.5625
110.410	732952.3125
109.202	867666.5625
107.993	771241.0625
106.785	681882.8125
105.577	697438.4375
104.369	688766.1875
103.160	464416.9375
101.952	486606.6875
100.744	476021.2188
99.536	391715.3750
98.327	306279.4063
97.119	260943.1250
95.911	213743.0938
94.703	247205.1563
93.494	47118.3633
92.286	72485.5547
91.078	37261.3711
89.870	112725.1797
88.661	13957.6611
87.453	2301.3230
86.245	-123904.9844
85.037	12983.5674
83.828	16403.6680
82.620	-9601.8643
81.412	149454.2188
80.204	13035.0254
78.995	-2693.5735
77.787	53209.9648
76.579	-12475.0742
75.371	17540.6211
74.162	46700.6719
72.954	43896.2969
71.746	26585.4668
70.538	29413.2422
69.329	40599.1250
68.121	-26683.1230
66.913	-33815.9883
65.705	-23999.7715
64.496	15008.8818
63.288	-23245.8457
62.080	-102989.3594
60.872	-158310.9375
59.663	-145335.4531
58.455	-197526.3906
57.247	-181023.2344
56.039	-190924.6250
54.830	-321284.5000
53.622	-103876.9141
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51.206	-340881.3125
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48.789	-173629.2500
47.581	-219526.8125
46.372	-145427.5781
45.164	-234324.8125
43.956	-232213.0313
42.748	-123677.7422
41.539	-272408.7500
40.331	-246968.8750
39.123	-103583.3203
37.915	-201443.0625
36.706	-131974.6875
35.498	-193934.9688
34.290	-224106.5000
33.082	0.0207
31.873	-167135.6563
30.665	-192115.6875
29.457	-239801.2344
28.249	-110939.6016
27.040	-150725.2656
25.832	-258087.6406
24.624	-197313.7813
23.416	-238842.6875
22.207	-134581.7188
20.999	-124484.4766
19.791	-62010.5938
18.583	-206745.1719
17.374	-164097.1250
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1.667	-110504.8281
0.459	-268329.7813
-0.749	-183901.6406
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-97.410	-286347.6250
-98.618	-281584.5313
-99.826	-159977.1406
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-104.659	-226562.7813
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-108.284	-178548.5000
-109.492	-134641.6094
-110.701	-122488.8516
-111.909	-192099.6875
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-114.325	-262827.7813
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-116.742	-237978.4375
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-119.158	-225857.9219
-120.367	-207894.6406
-121.575	-217808.0156
-122.783	-106037.8516
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-125.200	-198851.3594
-126.408	-209347.5000
-127.616	-194912.8281
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