The single crystal X-ray diffraction were carried out on beamline I19 at the Diamond Light Source in the UK using silicon double crystal monochromatic synchrotron radiation (λ = 0.6889 Å, Pilatus 2M detector).
The data were collected at five different temperatures, i.e., 100, 240, 300, 330, and 500 K.
Data reduction was performed with the CrysAlisPro (Version 171.40_64.53) software.
Files are readable in CrysAlisPro software which can be obtained free of charge upon registration at http://www.rigakuxrayforum.com/